Organocobaloximes with mixed-dioxime equatorial ligands: a one-pot synthesis

by Gupta, B. D.; Singh, V.; Qanungo, K.; Vijaikanth, V.; Yamuna, R.; Barclay, T.; Cordes, W.

BenzylCo(dmgH)(dpgH)Py has been synthesized by the reaction of benzyl chloride with a mixture of Co-1(dmgH)(2)Py and Co-1(dpgH)(2)Py, generated in situ, by the NaBH4 reduction of ClCo(dmgH)(2)Py and ClCo(dpgH)(2)Py. A mixture of three products is formed. The first crystal structure of an organocobaloxime with a mixed-dioxime ligand is reported.

Journal
Journal of Organometallic Chemistry
Volume
602
Issue
1-2
Year
2000
Start Page
1-4
URL
https://dx.doi.org/10.1016/s0022-328x(00)00105-4
ISBN/ISSN
1872-8561; 0022-328X
DOI
10.1016/s0022-328x(00)00105-4