Preparation and Solid-State Characterization of 4,4'-Bis(1,2,3,5-Dithiadiazolyl)

by Bryan, Clinton Dave; Cordes, A. Wallace; Haddon, Robert C.; Hicks, Robin G.; Oakley, Richard T.; Palstra, Thomas T. M.; Perel, Alexander J.

The reaction of oxamidrazone with sulfur dichloride affords 4,4'-bis(1,2,3,5-dithiadiazolium) dichloride, which can be reduced with triphenylantimony to the corresponding bis(1,2,3,5-dithiadiazolyl) diradical; the solid state structure and transport properties of the dimer [S2N2CCN2S2](2) are reported.

Journal
Journal of the Chemical Society-Chemical Communications
Issue
12
Year
1994
Start Page
1447
ISBN/ISSN
1364-548X; 0022-4936
DOI
10.1039/c39940001447